Abdollah Bashir-Hashemi - Mission Viejo CA Kurt Baum - Azusa CA
Assignee:
Fluorochem Inc. - Azusa CA
International Classification:
C07D27108
US Classification:
548125
Abstract:
The novel compound 3,3-Dinitro-4,4â-hydrozofurazan and the methods of preparation. The method of preparation 3,3-Dinitro-4,4â-hydrazofurazan which comprises partially reducing 3,3â-Dinitro-4,4â-azoxyfurazan. The method of preparing 3,3â-Dinitro-4,4â-hydrazofurazan by the partial reduction of 3,3â-Dinitro-4,4â-azofurazan.
A novel moisture curable polymer combination comprising, a member selected from the group consisting of a polydiolefin polymer containing olefinic unsaturation in either the main polymer backbone or in pendent side chains; and a loop polymer having a polymeric backbone and a plurality of olefinic groups which have been converted to closed loops by reaction with difunctional organic compounds reactive with said olefinic groups, said olefinic groups from which the loops are formed may either be present within the backbone and/or pendent from the polymeric backbone; and a silicon cross-linking compound containing at least one easily hydrolyzed substituent.
Substrates Having Moisture Curable Adherent Coating
Kurt Baum - Pasadena CA 91107 Wen-Huey Lin - Laguna Niguel CA 91677
International Classification:
B32B 2520
US Classification:
428447, 428450, 428500, 525100, 525479, 528 31
Abstract:
A novel moisture curable polymer combination comprising, a member selected from the group consisting of a polydiolefin polymer containing olefinic unsaturation in either the main polymer backbone or in pendent side chains; and a loop polymer having a polymeric backbone and a plurality of olefinic groups which have been converted to closed loops by reaction with difunctional organic compounds reactive with said olefinic groups, said olefinic groups from which the loops are formed may either be present within the backbone and/or pendent from the polymeric backbone; and a silicon crosslinking compound containing at least one easily hydrolyzed substituent.
Kurt Baum - Pasadena CA, US Wen-Huey Lin - Laguna Niguel CA, US
Assignee:
Flurochem, Inc. - Azusa CA
International Classification:
C07D 303/08 C07D 303/36 C07D 303/48
US Classification:
549551, 549558, 549563
Abstract:
The method of preparing novel allyl ethers. Novel glycidyl ethers and their preparation. Polyfunctional poly(glycidyl ethers) their methods of preparation. Novel polyurethanes based on the polyfunctional glycidyl ethers and their method of preparation.
Kurt Baum - Azusa CA, US Abdollah Bashir-Hashemi - Mission Viejo CA, US
International Classification:
C07D 271/08
US Classification:
548125
Abstract:
This invention consists of a method for converting diaminoglyoxime to diaminofurazan that can be carried out efficiently at about atmospheric pressure without the need for high pressure containment apparatus.This invention also consists of a method which comprises converting diaminoglyoxime to diaminofurazan at about atmospheric pressure in the presence of a strong base and/or an organic polar solvent.
Kurt Baum - Pasadena CA Vytautas Grakauskas - Arcadia CA Phillip T. Berkowitz - Woodbridge CT
Assignee:
The United States of America as represented by the Secretary of the Navy - Washington DC
International Classification:
C07D30508
US Classification:
549510
Abstract:
A process for preparing 3-hydroxyoxetane comprising the following steps in order (1) reacting a carboxylic acid of the formula CH. sub. 3 (CH. sub. 2). sub. n COOH with epichlorohydrin in the presence of anhydrous ferric chloride to produce an ester of the formula ##STR1## wherein n is an integer of from 0 to 3; (2) protecting the secondary hydroxy group of the ester with a blocking group, Z, that is stable to bases; thus forming a blocked ester of the formula ##STR2## (3) hydrolyzing the blocked ester formed in step (2) with an aqueous base to remove the carboxylic acid and form a 3-hydroxyoxetane derivative of the formula ##STR3## in which Z represents the blocking group; (4) removing the blocking group from the 3-hydroxyoxetane derivative by heating it with an alcohol and an acid to form the product 3-hydroxyoxetane, ##STR4##.
1,3-Diethynyladamantane And Methods Of Polymerization Thereof
Kurt Baum - Pasadena CA Thomas G. Archibald - Los Angeles CA
Assignee:
Fluorochem Inc. - Azusa CA
International Classification:
C08F 126
US Classification:
526282
Abstract:
1,3-Diethynyladamantane and a method of forming same by brominating adamantane to yield 1,3-dibromoadamantane, subjecting vinyl bromide to Friedel-Crafts alkylation with the 1,3-dibromoadamantane to form 1,3-bis(2,2-dibromoethyl)adamantane and subjecting the 1,3-bis(2,2-dibromoethyl)adamantane to dehydrohalogenation to yield the 1,3-diethynyladamantane. 1,3-Diethynyladamantane can be polymerized to produce strong, thermally stable resins suitable for advanced aerospace structural applications, as matrices for carbon-carbon systems and as electrical insulators. It can also be copolymerized with 1-ethynyladamantane to yield similarly useful resins.
Method Of Making And Polymerizing Perfluoroalkylene Acetylene Compounds
Kurt Baum - Pasadena CA Ronald O. Hunadi - Los Angeles CA Clifford D. Bedford - Mountain View CA
Assignee:
Fluorochem Inc. - Asuza CA
International Classification:
C07C 2122
US Classification:
570136
Abstract:
A perfluoroalkylene. alpha. ,. omega. -diacetylene compound having a fluorocarbon chain of from 5 to about 20 carbon atoms between two acetylene end groups, and a method of forming same by first reacting perfluoroalkylene diiodide having the formula I(CF. sub. 2). sub. n I, wherein n is a whole number from 5 to about 20, inclusive with bis(trimethylsilyl)acetylene, and converting the reaction product to the diacetylene with KF. The diacetylene has the general formula HC. tbd. C(CF. sub. 2). sub. n C. tbd. CH, wherein n is as set forth above, and it can be polymerized to produce a clear, hard, cross-linked resin suitable for use as a coating on bearings and in the manufacture of aircraft windshields. Monofunctional counterparts of the HC. tbd. C(CF. sub. 2). sub. n C. tbd. CH compounds can be formed by substituting perfluoroalkyl primary iodides for the diiodides in the above-described reaction.
Name / Title
Company / Classification
Phones & Addresses
Kurt Baum President
Fluorochem Inc Chemicals · Chemical Research Lab & Manufacture Organic Chemicals
680 S Ayon Ave, Azusa, CA 91702 680 S Ayon Ave, Duarte, CA 91702 626 334-6714