A process for preparing Anhydrous Betaine and Betaine Hydrochloride comprises treating a chloroacetic acid with sodium carbonate, and then dropping liquid trimethylamine to obtain Betaine products, wherein ion exchange resin and decompression process are utilized to assure the product having high purity and yield rate.
Creatinol O-Phosphate And Synthesis Method Thereof
Guoji Zhang - Tianjin, CN Jiashu Zhang - Diamond Bar CA, US
International Classification:
C07F 9/06 C07C 277/00
US Classification:
562 11, 564241
Abstract:
A creatinol O-phosphate is formed by chemically reacting a creatinol sulfate of creatinol compound with sulfuric acid to form a protected creatinol sulfate as a transition state of the synthesis process of the creatinol O-phosphate, wherein the protected creatinol is further reacted with one of PO, CIPOH, and POClto form the creatinol O-phosphate. The method of producing the protected creatinol sulfate includes a step of adding sulfuric acid into a creatinol sulfate to form a protected creatinol sulfate as the protected functional group. Therefore, the creatinol O-phosphate is formed by the process including the steps of chemically reacting the protected creatinol sulfate with one of POCl, CIPOOH, and POto form a creatinol O-phosphate solution; and crystallizing the creatinol O-phosphate solution to obtain crystallized creatinol O-phosphate.
Guoji Zhang - Tianjin, CN Jiashu Zhang - Diamond Bar CA, US
International Classification:
C07C 277/02
US Classification:
564241
Abstract:
A chemical compound of creatinol sulfate is formed by chemically reacting N-methyl-amino-ethanol, cyanamide, with sulfuric acid to produce the creatinol sulfate with relatively higher yield rate and purity, wherein the mol ratio of N-methyl-amino-ethanol, sulfuric acid, and cyanamide is approximately 2:1:2.
Method Of Producing N, N-Dimethyl Glycine Hydrochloride
A process for preparing N,N-Dimethyl Glycine Hydrochloride, comprises treating a chloroacetic acid with aqueous dimethylamine, and then dropping by hydrochloric acid to obtain N,N-dimethyl glycine as well as its hydrochloride salt, wherein decompression process is utilized to assure the product purity and active carbon is employed for cost saving aspect.
Isbn (Books And Publications)
Dian Fu Yu Jian Gou: Xin Wen Xie Zuo Yuan Li Tan Jiu